By Edward Allen
Describes systematically and in effectively usable shape the foundations through which sturdy architectural info are designed. the foundations are specified by eighty three short yet profusely illustrated ``detail patterns''. the 1st part examines all of the styles and illustrates numerous circumstances of its use. The latter half demonstrates the execution of those styles within the layout of key info for 3 assorted structures varieties. largely illustrated.
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92) . 1 Oxidative bromination of arenes, alkenes, and alkynes by using cat. NH4VO3/AlBr3/O2 system Entry 1 2 a Substrate Conditiona,b A, 60, 8 B, 60, 18 Product, isolated yield (%) 94 95 3 A, 60, 8 98 4 B, 110, 18 99 5 A, 40, 8 80 6 A, 80, 8 66 7 A, 120, 8 96 8 A, 120, 8 95 9 B, 110, 18 97 10 A, 60, 8 86c 11 A, 110, 18 Quant. 12 B, 120, 18 Quant. 5 mL of 1,4-dioxane, under atmospheric oxygen, 80 °C. 5 mL of ether, under atmospheric oxygen, rt. 5 mL of MeCN, under atmospheric oxygen, 80 °C c Together with 3-bromosalicylaldehde (11 %) d 120 mol% Bu4NBr was used as an additive e Reaction was conducted at 50 °C b T.